1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Base Information

Chemical Name:1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene
CAS No.:916843-99-7
Molecular Formula:C₂₄H₃₆O₂
Molecular Weight:356.549
Hs Code.:

Synonyms:1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

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Chemical Property of 1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

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Technology Process of 1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

There total 4 articles about 1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 13321-74-9
1-bromo-2,5-dimethoxy-4-methylbenzene

: 916843-99-7
1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Guidance literature:: 1-bromo-2,5-dimethoxy-4-methylbenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; at 0 ℃; for 0.25h;

farnesyl bromide; In diethyl ether; at 0 ℃;
DOI:10.1016/j.tetlet.2006.09.117

Reference yield:

: 24599-58-4
2,5-dimethoxy toluene

: 916843-99-7
1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 98 percent / AgO; HNO₃ / dioxane; H₂O / 20 °C

2.1: 61 percent / Me₃SiBr; Et₄NBF₄ / acetonitrile / 20 °C

3.1: 70 percent / NaOH / Heating

4.1: TMEDA; n-BuLi / diethyl ether / 0.25 h / 0 °C

4.2: 27 percent / diethyl ether / 0 °C

With silver(II) oxide; sodium hydroxide; n-butyllithium; trimethylsilyl bromide; N,N,N,N,-tetramethylethylenediamine; nitric acid; N,N,N,N-tetraethylammonium tetrafluoroborate; In 1,4-dioxane; diethyl ether; water; acetonitrile;
DOI:10.1016/j.tetlet.2006.09.117

Reference yield:

: 67289-05-8
2-bromo-5-methylbenzene-1,4-diol

: 916843-99-7
1,4-Dimethoxy-2-methyl-5-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / NaOH / Heating

2.1: TMEDA; n-BuLi / diethyl ether / 0.25 h / 0 °C

2.2: 27 percent / diethyl ether / 0 °C

With sodium hydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether;
DOI:10.1016/j.tetlet.2006.09.117