dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

Base Information

Chemical Name:dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate
CAS No.:132867-83-5
Molecular Formula:C₃₄H₃₂IO₉P
Molecular Weight:742.501
Hs Code.:

Synonyms:dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

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Technology Process of dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

There total 4 articles about dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1623-08-1
phosphoric acid dibenzyl ester

: 132867-81-3
2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl bromide

: 132867-83-5
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

Guidance literature:: silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; acetonitrile; Ambient temperature;
DOI:10.1016/0008-6215(91)80150-L

Reference yield:

: 132867-78-8
1,2,3-tri-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranose

: 132867-83-5
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 30percent hydrogen bromide / CH₂Cl₂; acetic acid / 5 h / Ambient temperature

2: 66 percent / silver trifluoromethane sulfonate / CH₂Cl₂; diethyl ether; acetonitrile / Ambient temperature

With hydrogen bromide; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/0008-6215(91)80150-L

Reference yield:

: 132867-76-6
1,2,3-tri-O-benzoyl-6-deoxy-α-L-galactopyranose

: 132867-83-5
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl) phophate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / dimethylformamide / Ambient temperature

2: 91 percent / 30percent hydrogen bromide / CH₂Cl₂; acetic acid / 5 h / Ambient temperature

3: 66 percent / silver trifluoromethane sulfonate / CH₂Cl₂; diethyl ether; acetonitrile / Ambient temperature

With hydrogen bromide; sodium iodide; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(91)80150-L