N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

Base Information

Chemical Name:N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide
CAS No.:1086378-85-9
Molecular Formula:C₁₅H₁₉N₃O₂S
Molecular Weight:305.401
Hs Code.:

Synonyms:N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

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Chemical Property of N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

Chemical Property:

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Technology Process of N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

There total 6 articles about N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1086378-82-6
N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carboxamide

: 1086378-85-9
N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

Guidance literature:: With tetraphosphorus decasulfide; In toluene; for 3h; Reflux;

Reference yield:

: 19155-88-5
benzo[c][1,2,5]oxadiazole-5-carboxylic acid

: 1086378-85-9
N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 2 h / Reflux

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 40 °C

3: tetraphosphorus decasulfide / toluene / 3 h / Reflux

With dmap; tetraphosphorus decasulfide; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 22348-44-3
trans-4-Methylamino-cyclohexanol

: 1086378-85-9
N-(trans-4-methoxycyclohexyl)-N-methyl-2,1,3-benzoxadiazole-5-carbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 2 h / Reflux

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 40 °C

3: tetraphosphorus decasulfide / toluene / 3 h / Reflux

With dmap; tetraphosphorus decasulfide; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;