tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate

Base Information

• Chemical Name: tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate
• CAS No.: 1186723-06-7
• Molecular Formula: C₂₂H₂₉NO₄
• Molecular Weight: 371.477

Synonyms:tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate

Chemical Property of tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate

There total 1 articles about tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

di-tert-butyl dicarbonate (24424-99-5) + 3-(5-(4-methoxyphenyl)pent-4-ynyl)piperidin-2-one (1186723-03-4) → tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate (1186723-06-7)

Guidance literature:

3-(5-(4-methoxyphenyl)pent-4-ynyl)piperidin-2-one; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -15 ℃; for 0.5h; Inert atmosphere;

di-tert-butyl dicarbonate; In tetrahydrofuran; hexane; at -78 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1021/jo901512m

Reference yield:

tert-butyl 3-(5-(4-methoxyphenyl)pent-4-ynyl)-2-oxopiperidine-1-carboxylate (1186723-06-7) → C22H31NO4

Guidance literature:

With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo901512m

upstream raw materials:

di-tert-butyl dicarbonate

3-(5-(4-methoxyphenyl)pent-4-ynyl)piperidin-2-one

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