C₁₅H₁₈O₄

Base Information

Chemical Name:C₁₅H₁₈O₄
CAS No.:1388153-23-8
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:

C<sub>15</sub>H<sub>18</sub>O<sub>4</sub>

Synonyms:C₁₅H₁₈O₄

Suppliers and Price of C₁₅H₁₈O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₅H₁₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₅H₁₈O₄

There total 6 articles about C₁₅H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1388152-90-6
C₁₆H₁₈O₅

: 1388153-23-8
C₁₅H₁₈O₄

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-89-3
C₁₄H₁₆O₄

: 1388153-23-8
C₁₅H₁₈O₄

Guidance literature:: Multi-step reaction with 3 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

3: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z

Reference yield:

: 1268269-18-6
C₁₄H₁₈O₃

: 1388153-23-8
C₁₅H₁₈O₄

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 0.75 h / 20 °C

2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

4: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

6: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z