Technology Process of C58H80N2Si4
There total 3 articles about C58H80N2Si4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(4-iPrC6H4)3SiNH2;
With
n-butyllithium;
In
diethyl ether; hexane;
at -35 ℃;
for 3h;
Inert atmosphere;
1,2-dichlorotetramethylsilane;
In
diethyl ether; hexane;
at -35 - 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ic300495k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium amide / tetrahydrofuran / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 3 h / -35 °C / Inert atmosphere
2.2: 16 h / -35 - 20 °C / Inert atmosphere
With
n-butyllithium; lithium amide;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ic300495k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / tetrahydrofuran / Inert atmosphere; Reflux
1.2: 48 h / -78 - 20 °C / Inert atmosphere; Reflux
2.1: lithium amide / tetrahydrofuran / Inert atmosphere
3.1: n-butyllithium / diethyl ether; hexane / 3 h / -35 °C / Inert atmosphere
3.2: 16 h / -35 - 20 °C / Inert atmosphere
With
n-butyllithium; lithium amide; magnesium;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ic300495k