C₃₂H₃₆O₈S

Base Information

Chemical Name:C₃₂H₃₆O₈S
CAS No.:1362110-57-3
Molecular Formula:C₃₂H₃₆O₈S
Molecular Weight:580.699
Hs Code.:

C<sub>32</sub>H<sub>36</sub>O<sub>8</sub>S

Synonyms:C₃₂H₃₆O₈S

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Chemical Property of C₃₂H₃₆O₈S

Chemical Property:

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Technology Process of C₃₂H₃₆O₈S

There total 13 articles about C₃₂H₃₆O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1362110-35-7
C₂₅H₃₂O₇

: 1005-56-7
phenylcarbonochloridothioate

: 1362110-57-3
C₃₂H₃₆O₈S

Guidance literature:: With pyridine; In acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-25-5
C₃₂H₄₇IO₄Si

: 1362110-57-3
C₃₂H₃₆O₈S

Guidance literature:: Multi-step reaction with 12 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: brine

2.1: Burgess Reagent / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

3.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

4.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

5.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

7.2: brine

8.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

9.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

11.1: ammonia / methanol; water / 6 h / 66 °C

11.2: 0 °C / pH 2

12.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; Burgess Reagent; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Barbier type cyclization / 8.1: Sharpless epoxidation;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-27-7
C₃₂H₄₆O₃Si

: 1362110-57-3
C₃₂H₃₆O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

3.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: brine

6.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

9.1: ammonia / methanol; water / 6 h / 66 °C

9.2: 0 °C / pH 2

10.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 6.1: Sharpless epoxidation;
DOI:10.1021/ol300390k