4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

Base Information

Chemical Name:4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride
CAS No.:80917-53-9
Molecular Formula:C₁₈H₁₆N₂O₂*ClH
Molecular Weight:328.798
Hs Code.:

4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenz<cd>indol-5(1H)-one hydrochloride

Synonyms:4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

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Chemical Property of 4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

Chemical Property:

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Technology Process of 4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

There total 5 articles about 4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 84131-93-1
4-azido-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

: 80917-53-9
4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 1h; under 3102.9 Torr;
DOI:10.1016/S0040-4020(01)80221-0

Reference yield:

: 132008-45-8,51867-02-8
1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

: 80917-53-9
4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / pyridine hydrobromide perbromide, acetic acid / 0.25 h / 50 °C

2: 58 percent / NaN₃, acetic acid / H₂O; dimethylformamide / 1 h / 20 °C

3: 2.22 g / concd. HCl / 10percent Pd/C / ethanol / 5 h / 20 °C

With hydrogenchloride; sodium azide; pyridinium hydrobromide perbromide; acetic acid; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00358a012

Reference yield:

: 51867-03-9
4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

: 80917-53-9
4-amino-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5(1H)-one hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaN₃, acetic acid / H₂O; dimethylformamide / 1 h / 20 °C

2: 2.22 g / concd. HCl / 10percent Pd/C / ethanol / 5 h / 20 °C

With hydrogenchloride; sodium azide; acetic acid; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00358a012