9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Base Information

Chemical Name:9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester
CAS No.:70801-92-2
Molecular Formula:C₃₇H₅₃NO₁₅
Molecular Weight:751.826
Hs Code.:

9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Synonyms:9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

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Chemical Property of 9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

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Technology Process of 9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

There total 13 articles about 9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 71048-95-8
ω-methoxycarbonyloctyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 5158-64-5
2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl bromide

: 70801-92-2
9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Guidance literature:: With mercury(II) cyanide; In acetonitrile; benzene; at 50 ℃;
DOI:10.1016/S0008-6215(82)80027-X

Reference yield:

: 56343-03-4,71048-95-8,79083-28-6,82863-54-5
9-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-nonanoic acid methyl ester

: 5158-64-5
2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl bromide

: 70801-92-2,82863-55-6,82950-99-0,146276-05-3
9-[(2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Guidance literature:: With mercury(II) cyanide; In acetonitrile; benzene; at 50 ℃; Yield given;
DOI:10.1016/S0008-6215(82)80027-X

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 70801-92-2
9-[(2R,4aR,6R,7R,8R,8aS)-7-Acetylamino-2-phenyl-8-((2S,3R,4R,5S,6S)-3,4,5-triacetoxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Hg(CN)2 / benzene / 25 °C

2: NaOMe / methanol

3: 87 percent / TsOH / 25 °C

4: 90 percent / Hg(CN)2 / benzene; acetonitrile / 50 °C

With sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; In methanol; acetonitrile; benzene;
DOI:10.1016/S0008-6215(82)80027-X