(S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

Base Information

Chemical Name:(S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate
CAS No.:1446270-37-6
Molecular Formula:C₁₃H₁₃N₃O₅S₂
Molecular Weight:355.395
Hs Code.:

Synonyms:(S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

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Chemical Property of (S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

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Technology Process of (S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

There total 2 articles about (S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 75-15-0,12122-00-8
carbon disulfide

: 2185-03-7
L-homoserine lactone hydrochloride

: 10147-71-4
2-chloro-N-(3-nitrophenyl)acetamide

: 1446270-37-6
(S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

Guidance literature:: carbon disulfide; L-homoserine lactone hydrochloride; With sodium phosphate dodecahydrate; In acetone; at 20 ℃; for 0.5h;

2-chloro-N-(3-nitrophenyl)acetamide; In acetone; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2013.05.035

Reference yield:

: 99-09-2
3-nitro-aniline

: 1446270-37-6
(S)-2-((3-nitrophenyl)amino)-2-oxoethyl (2-oxotetrahydrofuran-3-yl)carbamodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 20 °C

2.1: sodium phosphate dodecahydrate / acetone / 0.5 h / 20 °C

2.2: 0.5 h / 20 °C

With sodium phosphate dodecahydrate; potassium carbonate; In acetone;
DOI:10.1016/j.bmcl.2013.05.035