phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

Base Information

Chemical Name:phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone
CAS No.:94235-37-7
Molecular Formula:C₂₃H₂₈N₂O₂S
Molecular Weight:396.554
Hs Code.:

Synonyms:phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

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Technology Process of phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

There total 1 articles about phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 39692-51-8
phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 94235-37-7
phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

Guidance literature:: In methanol; for 0.0833333h; Heating;
DOI:10.1021/jo00205a007

Reference yield: 11.0%

: 94235-37-7
phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

: 94235-40-2
cis-1-phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)ethene

: 94235-39-9
trans-1-phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)ethene

Guidance literature:: With methyllithium; In various solvent(s); at 0 ℃; for 1h;
DOI:10.1021/jo00205a007

Reference yield:

: 94235-37-7
phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)methyl ketone tosylhydrazone

: 94235-38-8
1-diazo-1-phenyl 2-(2,3,3-trimethylcyclopenten-4-yl)ethane

Guidance literature:: With sodium hydride; Multistep reaction; 1.) diglyme, 5 min, 2.) petroleum ether, 110 deg C, 30 min;
DOI:10.1021/jo00205a007