N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

Base Information

Chemical Name:N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate
CAS No.:1160293-66-2
Molecular Formula:C₃₁H₄₃NO₇Si
Molecular Weight:569.77
Hs Code.:

Synonyms:N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

Suppliers and Price of N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

There total 1 articles about N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1160293-65-1
N,N-diethyl O-[2-iodo-4-(methoxymethoxy)-5-methoxy]-1-naphthyl-carbamate

: 137396-02-2
1-(3,5-bis((tert-butyldimethylsilyl)oxy)phenyl)ethanone

: 1160293-66-2
N,N-diethyl O-[1-isopropoxy-5-methoxymethoxy-2-(4-tert-butyldimethylsiloxy-2-methoxyphenyl)]-1-naphthylcarbamate

Guidance literature:: 1-(3,5-bis((tert-butyldimethylsilyl)oxy)phenyl)ethanone; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; Inert atmosphere;

N,N-diethyl O-[2-iodo-4-(methoxymethoxy)-5-methoxy]-1-naphthyl-carbamate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; hexane; at 20 ℃; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/jo9001454