(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

Base Information

Chemical Name:(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane
CAS No.:1380522-04-2
Molecular Formula:C₃₇H₅₀O₄Si
Molecular Weight:586.887
Hs Code.:

Synonyms:(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

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Chemical Property of (S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

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Technology Process of (S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

There total 2 articles about (S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6138-90-5
trans-geranyl bromide

: 1065484-10-7
(S)-1-(tert-butyldiphenylsilyloxy)-3-(4'-methoxybenzyloxy)propan-2-ol

: 1380522-04-2
(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;
DOI:10.1021/ja302099u

Reference yield:

: 109786-74-5
(R)-3-(4-methoxybenzyloxy)propane-1,2-diol

: 1380522-04-2
(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / 12 h / 0 - 20 °C

2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 20 °C

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja302099u

Reference yield:

: 1380522-04-2
(S,E)-tert-butyl(2-(3,7-dimethylocta-2,6-dienyloxy)-3-(4-methoxybenzyloxy)propoxy)diphenylsilane

: C₂₉H₄₂O₃Si

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 5 - 10 ℃; for 3h; pH=7; aq. phosphate buffer;
DOI:10.1021/ja302099u