(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Base Information

Chemical Name:(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine
CAS No.:112146-63-1
Molecular Formula:C₅₈H₁₀₁NO₄Si
Molecular Weight:904.53
Hs Code.:

Synonyms:(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Suppliers and Price of (2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

There total 15 articles about (2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 112146-62-0
(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoyl-1,3-di-O-(1-ethoxyethyl)-sphingenine

: 112146-63-1
(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Guidance literature:: With Amberlyst 15; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/0008-6215(87)80219-7

Reference yield: 61.0%

: 112146-62-0
(2S,3R,4E)-N-(2'S)-2'-tert-butyldiphenylsilyloxytetracosanoyl-1,3-di-O-(1-ethoxyethyl)-sphingenine

: 112146-63-1,112246-61-4
(2S,3R,4E)-N-(2'S)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Guidance literature:: With Amberlyst 15; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/0008-6215(87)80219-7

Reference yield:

: 2433-95-6,54563-86-9,54563-85-8
methyl (2R)-2-hydroxytetracosanoate

: 112146-63-1
(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoylsphingenine

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide / 24 h / 20 °C

2: 74 percent / NaOH / methanol; tetrahydrofuran / 16 h / 20 °C

3: 91 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / CH₂Cl₂ / 16 h / 20 °C

4: 67 percent / Amberlyst 15 / methanol; CH₂Cl₂ / 16 h / 20 °C

With 1H-imidazole; sodium hydroxide; Amberlyst 15; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80219-7