1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

Base Information

Chemical Name:1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate
CAS No.:317334-25-1
Molecular Formula:C₂HF₃O₂*C₁₈H₁₆N₂O₂S
Molecular Weight:438.427
Hs Code.:

Synonyms:1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

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Chemical Property of 1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

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Technology Process of 1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

There total 4 articles about 1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 317335-11-8
3-hydroxy-3-(1H-imidazol-2-yl)-1-(5-phenethylthiophen-2-yl)propan-1-one

: 317334-25-1
1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

Guidance literature:: With manganese(IV) oxide; In chloroform; at 20 ℃; for 5.5h;

Reference yield:

: 175203-54-0
1-(5-(phenylethynyl)thiophen-2-yl)ethanone

: 317334-25-1
1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / 5%-palladium/activated carbon / ethanol / 4 h / 20 °C / 760.05 Torr

2.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 1 h / -78 °C

2.2: 2.5 h / -78 - 20 °C

2.3: pH 9

3.1: triethylsilane; trifluoroacetic acid / 1 h / 20 °C

4.1: manganese(IV) oxide / chloroform / 5.5 h / 20 °C

With triethylsilane; manganese(IV) oxide; hydrogen; trifluoroacetic acid; lithium diisopropyl amide; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol; n-heptane; chloroform; ethylbenzene;

Reference yield:

: 317335-09-4
1-(5-phenethyl-[2]thienyl)-ethanone

: 317334-25-1
1-(1H-Imidazol-2-yl)-3-(5-phenethyl-thiophen-2-yl)propane-1,3-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 1 h / -78 °C

1.2: 2.5 h / -78 - 20 °C

1.3: pH 9

2.1: triethylsilane; trifluoroacetic acid / 1 h / 20 °C

3.1: manganese(IV) oxide / chloroform / 5.5 h / 20 °C

With triethylsilane; manganese(IV) oxide; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; chloroform; ethylbenzene;