N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine

Base Information

• Chemical Name: N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine
• CAS No.: 253877-77-9
• Molecular Formula: C₃₃H₅₆N₄O₆
• Molecular Weight: 604.831

Synonyms:N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine

Chemical Property of N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine

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Technology Process of N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine

There total 5 articles about N₁-(tert-butocycarbonyl)-N₂₂-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(tert-butoxycarbonylamino)hexanoic acid (6404-29-1) → N1-(tert-butocycarbonyl)-N22-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine (253877-77-9)

Guidance literature:

Multi-step reaction with 4 steps

1: Et₃N / dioxane / 0.5 h / 5 °C

2: dioxane / 20 °C

3: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.75 h / 20 °C / 775.72 Torr

4: dioxane / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; 1: Acetoxylation / 2: Condensation / 3: Catalytic hydrogenation / 4: Condensation;

DOI:10.1021/jm991110n

Reference yield:

C14H25NO6 (219117-92-7) → N1-(tert-butocycarbonyl)-N22-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine (253877-77-9)

Guidance literature:

Multi-step reaction with 3 steps

1: dioxane / 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.75 h / 20 °C / 775.72 Torr

3: dioxane / 20 °C

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; 1: Condensation / 2: Catalytic hydrogenation / 3: Condensation;

DOI:10.1021/jm991110n

Reference yield:

N1-(tert-butoxycarbonyl)-N15-[(benzyloxy)carbonyl]-6-oxo-7-aza-1,15-pentadecanediamine (253877-76-8) → N1-(tert-butocycarbonyl)-N22-[(benzyloxy)carbonyl]-6,17-dioxo-7,16-diaza-1,22-docosanediamine (253877-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.75 h / 20 °C / 775.72 Torr

2: dioxane / 20 °C

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; 1: Catalytic hydrogenation / 2: Condensation;

DOI:10.1021/jm991110n

upstream raw materials:

N₁-(tert-butoxycarbonyl)-6-oxo-7-aza-1,15-pentadecanediamine

6-(tert-butoxycarbonylamino)hexanoic acid

6-(benzyloxycarbonylamino)hexanoic acid

C₁₄H₂₅NO₆

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