(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

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Chemical Name:(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine
CAS No.:1043481-68-0
Molecular Formula:C₁₇H₂₆N₂O₂
Molecular Weight:290.406
Hs Code.:

Synonyms:(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

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Technology Process of (2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

There total 1 articles about (2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 80928-05-8,137819-87-5
(R)-(+)-2-Benzyloxybutyraldehyde

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 1043481-68-0
(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.tetasy.2008.04.021

Reference yield: 44.0%

: 1043481-68-0
(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine

: 76-63-1
allytriphenyltin

: 814-68-6,25189-84-8
acryloyl chloride

: 1043481-73-7
(1R,1R,2S)-(-)-N-[1-(1-benzyloxypropyl)but-3-enyl]-N-(2-methoxymethylpyrrolidin-1-yl)acrylamide

Guidance literature:: allytriphenyltin; With phenyllithium; In diethyl ether; at 20 ℃; for 0.5h;

(2R,2S)-(-)-(E)-N-(2-benzyloxybutylidene)-N-(2-methoxymethylpyrrolidin-1-yl)amine; In diethyl ether; at -78 - 20 ℃; for 12h;

acryloyl chloride; In diethyl ether; at -78 - 20 ℃; for 3h; Further stages.;
DOI:10.1016/j.tetasy.2008.04.021