methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Base Information

Chemical Name:methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten
CAS No.:1429466-30-7
Molecular Formula:C₁₉H₁₅O₇PW
Molecular Weight:570.148
Hs Code.:

Synonyms:methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Suppliers and Price of methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

There total 4 articles about methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₂₄H₁₅O₁₁PW₂

: 1429466-30-7
methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Guidance literature:: With dimethyl sulfoxide; In toluene; at 50 ℃; Inert atmosphere;
DOI:10.1021/om400109h

Reference yield:

: C₂₃H₁₂O₁₁PW₂^(1-)*Li⁽¹⁺⁾

: 1429466-30-7
methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; hexane / 20 °C / Inert atmosphere

2: dimethyl sulfoxide / toluene / 50 °C / Inert atmosphere

With dimethyl sulfoxide; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/om400109h

Reference yield:

: 14040-11-0
tungsten hexacarbonyl

: 1429466-30-7
methyl 3,4-dimethyl-1-phenyl-1H-phosphole-2-carboxylate tungsten

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 - -90 °C / Inert atmosphere

1.2: 0.5 h / -90 °C / Inert atmosphere

2.1: tetrahydrofuran; hexane / 20 °C / Inert atmosphere

3.1: dimethyl sulfoxide / toluene / 50 °C / Inert atmosphere

With n-butyllithium; dimethyl sulfoxide; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/om400109h