(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆

Base Information

• Chemical Name: (C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆
• CAS No.: 84369-22-2
• Molecular Formula: C₄₂H₃₇NO₂P₂Re*F₆P
• Molecular Weight: 980.88

Synonyms:(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆

Chemical Property of (C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆

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Technology Process of (C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆

There total 1 articles about (C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(C₆H₅)3)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(C5H5)Re(NO)(P(C6H5)3)(CH2O)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(CH2O)PF6 (84369-16-4) → (C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)PF6 (84369-22-2)

Guidance literature:

With PPh₃; In dichloromethane; the formyl complex and PPh3 (molar ratio 1:2) were dissolved in CH2Cl2 under N2; crystn. by vapor diffusion (ether), washing (ether), drying in vac., elem. anal.;

Reference yield: 64.0%

carbonyl(cyclopentadienyl)(trimethylphosphane)cobalt (66652-86-6) + (C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)PF6 (84369-22-2) → Co(Cp)(carbonyl)(triphenylphosphine) + (C5H5)Re(NO)(P(C6H5)3)(OCH2P(CH3)3)(1+)*PF6(1-)*CH2Cl2=(C5H5)Re(NO)(P(C6H5)3)(OCH2P(CH3)3)PF6*CH2Cl2 (100815-23-4) + (C5H5)Re(NO)(P(C6H5)3)(OC(C(2)H3)2)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(OC(C(2)H3)2)PF6 (100815-25-6)

Guidance literature:

In [⁽²⁾H₆]acetone; a NMR tube was charged under N2 with equimolar amts. of Re and Co complexes, Ph3SiMe standard and acetone-d6 and kept at room temp. for 16 h; identified by IR and NMR spectra;

Reference yield:

(C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(OCH2P(C6H5)3)PF6 (84369-22-2) → (C5H5)Re(NO)(P(C6H5)3)(CH2O)(1+)*PF6(1-)=(C5H5)Re(NO)(P(C6H5)3)(CH2O)PF6 (84369-16-4)

Guidance literature:

In acetone; equilibrum in acetone soln. (84:16);

DOI:10.1021/ja00342a070

upstream raw materials:

(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

Downstream raw materials:

(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(CH₂O)PF₆

(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(CH₃)3)⁽¹⁺⁾*PF₆^(1-)*CH₂Cl₂=(C₅H₅)Re(NO)(P(C₆H₅)3)(OCH₂P(CH₃)3)PF₆*CH₂Cl₂

(C₅H₅)Re(NO)(P(C₆H₅)3)(OC(C⁽²⁾H₃)2)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)Re(NO)(P(C₆H₅)3)(OC(C⁽²⁾H₃)2)PF₆

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