α,ε-N,N'-dibenzoyllysine methyl ester

Base Information

Chemical Name:α,ε-N,N'-dibenzoyllysine methyl ester
CAS No.:133787-17-4
Molecular Formula:C₂₁H₂₄N₂O₄
Molecular Weight:368.433
Hs Code.:

Synonyms:α,ε-N,N'-dibenzoyllysine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α,ε-N,N'-dibenzoyllysine methyl ester

Chemical Property:

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Technology Process of α,ε-N,N'-dibenzoyllysine methyl ester

There total 3 articles about α,ε-N,N'-dibenzoyllysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 135789-87-6,114968-97-7
phosphonic acid diethyl ester

: 714222-56-7
(+/-)-methyl N^α,N^ε-dibenzoyl-α-formyllysinate

: 133787-17-4
α,ε-N,N'-dibenzoyllysine methyl ester

: 714222-62-5
(+/-)-methyl N^α,N^ε-dibenzoyl-α-(E)-(2'-fluoro-2'-benzenesulfonyl)vinyllysinate

Guidance literature:: phosphonic acid diethyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

(+/-)-methyl N^α,N^ε-dibenzoyl-α-formyllysinate; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/ol049422u

Reference yield:

: 74761-86-7
Methyl N^α,N^ε-dibenzoyl-2-vinyllysinate

: 133787-17-4
α,ε-N,N'-dibenzoyllysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: ozone / CH₂Cl₂ / -78 °C

1.2: 84 percent / acetic acid; Zn / CH₂Cl₂ / Heating

2.1: LiHMDS / tetrahydrofuran / 0.5 h / -78 °C

2.2: 24 percent / tetrahydrofuran / -78 - 20 °C

With ozone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol049422u