α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

Base Information

Chemical Name:α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane
CAS No.:1262392-80-2
Molecular Formula:C₃₂H₃₃N₃O₄
Molecular Weight:523.632
Hs Code.:

Synonyms:α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

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Chemical Property of α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

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Technology Process of α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

There total 5 articles about α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1262392-79-9
4-(6-(N-methyl(N-phenyl)amino)hexyloxy)biphenyl-4'-ol

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1262392-80-2
α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

Guidance literature:: 4-amino-benzoic acid; With sulfuric acid; acetic acid; sodium nitrite; In water; for 0.166667h; Cooling with ice;

4-(6-(N-methyl(N-phenyl)amino)hexyloxy)biphenyl-4'-ol; In N,N-dimethyl-formamide; at 0 - 5 ℃;
DOI:10.1039/c0jm02228d

Reference yield:

: 100-61-8
N-methylaniline

: 1262392-80-2
α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 5 h / 80 °C

2.1: trichlorophosphate / 0 - 110 °C / Cooling with ice

3.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 80 °C

4.1: sulfuric acid; acetic acid; sodium nitrite / water / 0.17 h / Cooling with ice

4.2: 0 - 5 °C

With sulfuric acid; potassium carbonate; acetic acid; potassium iodide; sodium nitrite; trichlorophosphate; In water; N,N-dimethyl-formamide;
DOI:10.1039/c0jm02228d

Reference yield:

: N-(6-chlorohexyl)-N-methylaniline

: 1262392-80-2
α-(N-methyl-N-(4-(4'-carboxyphenylazo)phenyl)amino)-ω-(4-hydroxylbiphenylene)-hexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 80 °C

2.1: sulfuric acid; acetic acid; sodium nitrite / water / 0.17 h / Cooling with ice

2.2: 0 - 5 °C

With sulfuric acid; potassium carbonate; acetic acid; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1039/c0jm02228d