C₂₈H₂₄I₂

Base Information

Chemical Name:C₂₈H₂₄I₂
CAS No.:1267662-12-3
Molecular Formula:C₂₈H₂₄I₂
Molecular Weight:614.308
Hs Code.:

C<sub>28</sub>H<sub>24</sub>I<sub>2</sub>

Synonyms:C₂₈H₂₄I₂

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Chemical Property of C₂₈H₂₄I₂

Chemical Property:

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Technology Process of C₂₈H₂₄I₂

There total 7 articles about C₂₈H₂₄I₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1267662-11-2
C₃₄H₄₂Si₂

: 1267662-12-3
C₂₈H₂₄I₂

Guidance literature:: With Iodine monochloride; In dichloromethane; at 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/chem.201002574

Reference yield:

: 1611-92-3
3,5-dibromotoluene

: 1267662-12-3
C₂₈H₂₄I₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / diethyl ether; hexane / 1.17 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: dichloromethane / 1 h / Inert atmosphere; Reflux

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / Inert atmosphere; Reflux

5.1: Iodine monochloride / dichloromethane / 2.5 h / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Iodine monochloride; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water;
DOI:10.1002/chem.201002574

Reference yield:

: 315668-55-4
3-bromo-5-trimethysilyltoluene

: 1267662-12-3
C₂₈H₂₄I₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dichloromethane / 1 h / Inert atmosphere; Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / Inert atmosphere; Reflux

4.1: Iodine monochloride / dichloromethane / 2.5 h / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Iodine monochloride; sodium hydrogencarbonate; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1002/chem.201002574