(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate
CAS No.:210428-05-0
Molecular Formula:C₃₁H₃₉NO₅Si
Molecular Weight:533.74
Hs Code.:

Synonyms:(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

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Technology Process of (S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

There total 4 articles about (S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 58479-61-1
tert-butylchlorodiphenylsilane

: 210428-05-0
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 210428-05-0
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaHCO₃ / CH₂Cl₂ / 2 h / Ambient temperature

2: 89 percent / imidazole / CH₂Cl₂ / 4 h / Ambient temperature

With 1H-imidazole; sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

: 210428-05-0
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldiphenylsilyloxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / 24 h / Ambient temperature

2: 93 percent / NaHCO₃ / CH₂Cl₂ / 2 h / Ambient temperature

3: 89 percent / imidazole / CH₂Cl₂ / 4 h / Ambient temperature

With 1H-imidazole; hydrogenchloride; sodium hydrogencarbonate; In dichloromethane;