F₃SiSiH₃

Base Information

• Chemical Name: F₃SiSiH₃
• CAS No.: 15195-26-3
• Molecular Formula: F₃H₃Si₂
• Molecular Weight: 116.19
• Mol file: 15195-26-3.mol

Synonyms:F₃SiSiH₃

Chemical Property of F₃SiSiH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of F₃SiSiH₃

There total 10 articles about F₃SiSiH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

SiF3SiHBr2 (56144-86-6) + trimethylstannane (1631-73-8) → F3SiSiH3 (15195-26-3) + trimethyltin bromide (1066-44-0)

Guidance literature:

In neat (no solvent); Warming of starting materials (in absence of solvent, vac. line) for 30 min to room temp.; Removal of Me3SnBr by passing the mixt. through a trap cooled to -95°C (toluene), IR and NMR identification of volatile resulting compd.;

Reference yield: 90.0%

SiF3SiFHBr (56144-87-7) + trimethylstannane (1631-73-8) → SiF3SiF2H (24628-33-9) + F3SiSiH3 (15195-26-3) + trimethyltin bromide (1066-44-0)

Guidance literature:

In neat (no solvent); React. (vac. line, no solvent) at room temp. for 10 min.; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). IR and NMR spectra indicate presence of resulting compounds in approximately equimolar amt.;

Reference yield: 90.0%

SiF2HSiF2Cl (119895-86-2) + trimethylstannane (1631-73-8) → SiF3SiF2H (24628-33-9) + F3SiSiH3 (15195-26-3) + trimethyltin bromide (1066-44-0)

Guidance literature:

In neat (no solvent); React. of equimolar amt. of starting materials (vac. line, room temp., 10 min).; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). IR identificatio of resulting compounds.;

upstream raw materials:

SiF₃SiHBr₂

trimethylstannane

polytetrafluoroethylene

SiF₃SiFHBr