(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

Base Information

Chemical Name:(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide
CAS No.:133941-12-5
Molecular Formula:C₁₈H₂₁N₃O₂
Molecular Weight:311.384
Hs Code.:

Synonyms:(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

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Chemical Property of (+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

Chemical Property:

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Technology Process of (+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

There total 3 articles about (+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 133941-11-4
(+/-)-trans-3-(aminocarbonyl)-1-<3-oxo-3-<(2-phenylcyclopropyl)amino>propyl>pyridinium bromide

: 133941-12-5
(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In water; ethyl acetate;
DOI:10.1002/jps.2600800313

Reference yield:

: 1986-47-6,2208-35-7,2337-86-2,4548-34-9,37388-05-9,54779-58-7,61-81-4
tranylcypromine hydrochloride

: 133941-12-5
(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Na₂CO₃, DCC / dimethylformamide / 48 h / Ambient temperature

2: 65 percent / Na₂S₂O₄, NaHCO₃ / H₂O; ethyl acetate

With sodium dithionite; sodium hydrogencarbonate; sodium carbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600800313

Reference yield:

: 109822-09-5
3-carbamoyl-1-carboxyethyl pyridinium bromide

: 133941-12-5
(+/-)-trans-3-(aminocarbonyl)-N-(2-phenylcyclopropyl)-1(4H)-pyridinepropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Na₂CO₃, DCC / dimethylformamide / 48 h / Ambient temperature

2: 65 percent / Na₂S₂O₄, NaHCO₃ / H₂O; ethyl acetate

With sodium dithionite; sodium hydrogencarbonate; sodium carbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600800313