13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Base Information

Chemical Name:13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane
CAS No.:71089-11-7
Molecular Formula:C17H27 N O4
Molecular Weight:309.406
Hs Code.:
DSSTox Substance ID:DTXSID20221311
Nikkaji Number:J488.649F
Wikidata:Q83099042
ChEMBL ID:CHEMBL373818
Mol file:71089-11-7.mol

Synonyms:benzyl-aza-15-crown-5;benzylaza-15-crown-5

Suppliers and Price of 13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BENZYLAZA-15-CROWN-5 95.00%
5MG
$ 498.36

Total 4 raw suppliers

Chemical Property of 13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Chemical Property:

Vapor Pressure:1.03E-07mmHg at 25°C
Boiling Point:433.4°C at 760 mmHg
Flash Point:124.8°C
PSA：40.16000
Density:1.032g/cm³
LogP:1.50650
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:309.19400834
Heavy Atom Count:22
Complexity:243

Purity/Quality:

99% ^*data from raw suppliers

BENZYLAZA-15-CROWN-5 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOCCOCCOCCN1CC2=CC=CC=C2

Technology Process of 13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

There total 10 articles about 13-(Phenylmethyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 41024-91-3
penta(ethylene glycol) bis(p-toluenesulfonate)

: 100-46-9
benzylamine

: 71089-11-7
1-benzyl-1-aza-15-crown-5

Guidance literature:: With sodium carbonate; In toluene; for 3h; Heating;
DOI:10.1021/jo961098w

Reference yield: 82.0%

: 101-32-6
N-benzyl-diethanolamine

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 71089-11-7
1-benzyl-1-aza-15-crown-5

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In water; toluene; at 70 ℃; for 10h; Inert atmosphere;
DOI:10.1039/c9dt01512d

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 71089-11-7
1-benzyl-1-aza-15-crown-5

Guidance literature:: Multi-step reaction with 3 steps

1: (i) NaH, THF, (ii) /BRN= 632509/

2: LiAlH₄ / tetrahydrofuran / Heating

3: K₂CO₃ / acetonitrile

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1039/P19790000357