C₂₄H₁₅NO

Base Information

Chemical Name:C₂₄H₁₅NO
CAS No.:187238-37-5
Molecular Formula:C₂₄H₁₅NO
Molecular Weight:333.389
Hs Code.:

Synonyms:C₂₄H₁₅NO

Suppliers and Price of C₂₄H₁₅NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₁₅NO

Chemical Property:

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Technology Process of C₂₄H₁₅NO

There total 5 articles about C₂₄H₁₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3058-39-7
4-iodobenzonitrile

: 191094-20-9
1-ethynyl-4-((4-methoxyphenyl)ethynyl)benzene

: 187238-37-5
C₂₄H₁₅NO

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In toluene; at 55 ℃; Inert atmosphere;
DOI:10.1246/cl.140579

Reference yield:

: 696-62-8
para-iodoanisole

: 187238-37-5
C₂₄H₁₅NO

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; copper(l) iodide / toluene / 55 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; copper(l) iodide / toluene / 55 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; toluene; 1: |Sonogashira Cross-Coupling / 3: |Sonogashira Cross-Coupling;
DOI:10.1246/cl.140579

Reference yield:

: C₂₅H₂₃OPSi

: 187238-37-5
C₂₄H₁₅NO

Guidance literature:: Multi-step reaction with 4 steps

1: methylmagnesium bromide / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; copper(l) iodide / toluene / 55 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; copper(l) iodide / toluene / 55 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; methylmagnesium bromide; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; toluene; 2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
DOI:10.1246/cl.140579