Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

Base Information

Chemical Name:Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester
CAS No.:201025-92-5
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

Synonyms:Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

Suppliers and Price of Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

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Technology Process of Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

There total 2 articles about Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 103-71-9
phenyl isocyanate

: 74457-10-6
anti-1,5-dimethylbicyclo[3.2.1]octan-8-ol

: 201025-92-5
Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

Guidance literature:: In Petroleum ether; at 120 ℃; for 4h;
DOI:10.1016/S0040-4020(97)10148-X

Reference yield:

: 74457-07-1
anti-8-acetoxy-1,5-dimethykbicyclo[3.2.1]octane

: 201025-92-5
Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / KHCO₃ / methanol

2: 83 percent / petroleum ether / 4 h / 120 °C

With potassium hydrogencarbonate; In methanol; Petroleum ether;
DOI:10.1016/S0040-4020(97)10148-X

Reference yield:

: 201025-92-5
Phenyl-carbamic acid (1R,5S,8R)-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

: Phenyl-carbamic acid (1S,3S,5R,8S)-3-hydroxy-1,5-dimethyl-bicyclo[3.2.1]oct-8-yl ester

: Phenyl-carbamic acid (1S,5R,8S)-1,5-dimethyl-3-oxo-bicyclo[3.2.1]oct-8-yl ester

Guidance literature:: With Beauveria bassiana; Product distribution; selectivity of biooxygenation of N-phenylcarbamates by the fungus Beauveria bassiana;
DOI:10.1016/S0040-4020(97)10148-X