<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

Base Information

Chemical Name:<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester
CAS No.:154921-13-8
Molecular Formula:C₂₆H₃₀I₃N₃O₁₃
Molecular Weight:973.25
Hs Code.:

Synonyms:<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

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Chemical Property of <3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

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Technology Process of <3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

There total 6 articles about <3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: N,N'-bis<2-hydroxy-1-(hydroxymethyl)ethyl>-2,4,6-triiodo-5-<4-(hydroxymethyl)-2-oxo-3-oxazolidinyl>-1,3-benzenedicarboxamide

: 154921-13-8
<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

Guidance literature:

Reference yield:

: 35453-19-1
2,4,6-triiodo-5-aminoisophthalic acid

: 154921-13-8
<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / thionyl chloride

2: N,N-dimethyl-acetamide / 16 h / Ambient temperature

3: pyridine / 6 h / Ambient temperature

4: dioxane; toluene / 15 h / 60 °C

5: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

With pyridine; thionyl chloride; phenylmercuric acetate; In 1,4-dioxane; N,N-dimethyl acetamide; toluene;
DOI:10.1021/jo00085a023

Reference yield:

: 99-31-0
5-aminoisophthalic acid

: 154921-13-8
<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 74 percent / aq. potassium iododichloride / H₂O / 18 h / 55 - 60 °C

2: 92 percent / thionyl chloride

3: N,N-dimethyl-acetamide / 16 h / Ambient temperature

4: pyridine / 6 h / Ambient temperature

5: dioxane; toluene / 15 h / 60 °C

6: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

With pyridine; thionyl chloride; potassium dichloroiodate; phenylmercuric acetate; In 1,4-dioxane; N,N-dimethyl acetamide; water; toluene;
DOI:10.1021/jo00085a023