dimethyl 3-isopropylglutarate

Base Information

Chemical Name:dimethyl 3-isopropylglutarate
CAS No.:2338-44-5
Molecular Formula:C₁₀H₁₈O₄
Molecular Weight:202.251
Hs Code.:

Synonyms:dimethyl 3-isopropylglutarate

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Chemical Property of dimethyl 3-isopropylglutarate

Chemical Property:

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Technology Process of dimethyl 3-isopropylglutarate

There total 1 articles about dimethyl 3-isopropylglutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5164-76-1
dimethyl glutaconate

: 2338-44-5
dimethyl 3-isopropylglutarate

Guidance literature:: i-C₃H₇MgX; With copper(l) iodide; In tetrahydrofuran; at 20 ℃;

dimethyl glutaconate; With chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jm050033v

Reference yield:

: 2338-44-5
dimethyl 3-isopropylglutarate

: 4165-99-5
3-isopropylglutaric acid

Guidance literature:: With potassium hydroxide;

Reference yield:

: 2338-44-5
dimethyl 3-isopropylglutarate

: toluene-4-sulfonic acid 3-[2-(4'-chloro-biphenyl-4-yloxy)-ethyl]-4-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating

2: pyridine / 2 h / 20 °C

3: K₂CO₃ / acetonitrile / 24 h / 60 °C

With pyridine; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm050033v