3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

Base Information

Chemical Name:3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol
CAS No.:260370-07-8
Molecular Formula:C₃₁H₃₃NO₂
Molecular Weight:451.609
Hs Code.:

Synonyms:3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

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Chemical Property of 3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

Chemical Property:

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Technology Process of 3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

There total 1 articles about 3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 108-86-1,52753-63-6
bromobenzene

: 105-71-5
3-methyl[(3-methoxy-3-oxopropyl)methylamino]propanoate

: 260370-07-8
3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

Guidance literature:: bromobenzene; With lithium; In diethyl ether;

3-methyl[(3-methoxy-3-oxopropyl)methylamino]propanoate; In diethyl ether; at 0 - 20 ℃;
DOI:10.1139/v00-001

Reference yield: 90.0%

: 24356-01-2
tetrabenzylzirconium(IV)

: 260370-07-8
3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

: cis,fac-Zr[MeN(CH₂CH₂C(O)Ph₂)2]2

Guidance literature:: In toluene; stirring for 1 h; volatiles were removed under pressure, recrystn. from a mixt. of toluene and hexane; elem. anal.;
DOI:10.1139/v00-001

Reference yield: 85.0%

: 24356-01-2
tetrabenzylzirconium(IV)

: 260370-07-8
3-[(3-hydroxy-3,3-diphenyl-propyl)-methyl-amino]-1,1-diphenyl-propan-1-ol

: 260370-14-7
Zr[MeN(CH₂CH₂C(O)Ph₂)2][CH₂Ph]2

Guidance literature:: In toluene; under Ar atm. soln. HOCPh2CH2CH2NMeCH2CH2CPh2OH in toluene was added dropwise at -78°C to soln. tetrabenzylzirconium in toluene, mixt. was stirred for 30 min; solvent was removed in vacuo, residue was recrystd. from toluene-hexane; elem. anal.;
DOI:10.1021/om9907324