6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

Base Information

Chemical Name:6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid
CAS No.:124895-47-2
Molecular Formula:C₂₂H₂₂O₅
Molecular Weight:366.414
Hs Code.:

Synonyms:6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

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Chemical Property of 6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

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Technology Process of 6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

There total 1 articles about 6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124895-46-1
4-(benzyloxy)-2-isopropyl-3-methoxybenzaldehyde

: 123-25-1
succinic acid diethyl ester

: 124895-47-2
6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

Guidance literature:: With sodium hydroxide; potassium tert-butylate; sodium acetate; acetic anhydride; Yield given. Multistep reaction; 1.) t-BuOH, reflux, 45 min, 2.) AcOH, reflux, 3.) MeOH, reflux;
DOI:10.1002/hlca.19890720221

Reference yield: 82.0%

: 124895-47-2
6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

: 124895-48-3
7-(benzyloxy)-3-(hydroxymethyl)-5-isopropyl-6-methoxy-1-naphthol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1002/hlca.19890720221

Reference yield:

: 124895-47-2
6-(benzyloxy)-4-hydroxy-8-isopropyl-7-methoxynaphthalene-2-carboxylic acid

: 124895-49-4
7,7'-bis(benzyloxy)-3,3'-bis(hydroxymethyl)-5,5'-diisopropyl-6,6'-dimethoxy<2,2'-binaphthalene>-1,1'-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

2: 83 percent / (t-Bu)2O₂ / chlorobenzene / 9 h / Heating

With lithium aluminium tetrahydride; di-tert-butyl peroxide; In tetrahydrofuran; chlorobenzene;
DOI:10.1002/hlca.19890720221