(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

Base Information

Chemical Name:(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester
CAS No.:202867-95-6
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:

Synonyms:(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

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Chemical Property of (1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

Chemical Property:

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Technology Process of (1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

There total 4 articles about (1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₉NO₄

: 100-51-6,185532-71-2
benzyl alcohol

: 202867-95-6
(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

Guidance literature:: C₁₁H₁₉NO₄; In benzene; for 2h; Heating / reflux;

benzyl alcohol; With triethylamine; In dichloromethane; benzene; for 16h; Heating / reflux;

Reference yield:

: cis-2-methoxycarbonylcyclohexane-1-carboxylic acid

: 202867-95-6
(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 1 h / -20 °C

2: aq. NaN₃ / tetrahydrofuran / 2 h / 20 °C

3: benzene / 2 h / Heating

4: Et₃N / CH₂Cl₂ / 4.5 h / Heating

With sodium azide; triethylamine; In tetrahydrofuran; dichloromethane; benzene; 3: Curtius degradation;
DOI:10.1055/s-2001-16745

Reference yield:

: 2-azidocarbonyl-cyclohexanecarboxylic acid methyl ester

: 202867-95-6
(1R,2S)-2-Benzyloxycarbonylamino-cyclohexane-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 2 h / Heating

2: Et₃N / CH₂Cl₂ / 4.5 h / Heating

With triethylamine; In dichloromethane; benzene; 1: Curtius degradation;
DOI:10.1055/s-2001-16745