2-(6-chrysenyl)cyclohexanol

Base Information

Chemical Name:2-(6-chrysenyl)cyclohexanol
CAS No.:111209-23-5
Molecular Formula:C₂₄H₂₂O
Molecular Weight:326.438
Hs Code.:

Synonyms:2-(6-chrysenyl)cyclohexanol

Suppliers and Price of 2-(6-chrysenyl)cyclohexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(6-chrysenyl)cyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(6-chrysenyl)cyclohexanol

There total 2 articles about 2-(6-chrysenyl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7397-93-5
6-bromochrysene

: 286-20-4
cyclohexane-1,2-epoxide

: 111209-23-5
2-(6-chrysenyl)cyclohexanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, ether, 2 h, 2.) ether, overnight;
DOI:10.1021/jo00235a005

Reference yield:

: 218-01-9
chrysene

: 111209-23-5
2-(6-chrysenyl)cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / CS₂ / 48 h / 40 °C

2: 1.) n-butyllithium / 1.) hexane, ether, 2 h, 2.) ether, overnight

With n-butyllithium; bromine; In carbon disulfide;
DOI:10.1021/jo00235a005

Reference yield:

: 111209-23-5
2-(6-chrysenyl)cyclohexanol

: 111189-32-3
naphtho[1,2-b]fluoranthene

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / pyridinium dichromate / dimethylformamide / Ambient temperature

2: 1.) polyphosphoric acid (PPA), 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) 110 deg C, 2 h, 2.) benzene, reflux, 30 min

With dipyridinium dichromate; PPA; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In N,N-dimethyl-formamide;
DOI:10.1021/jo00235a005