C₂₃H₃₃N₃O₃Si

Base Information

Chemical Name:C₂₃H₃₃N₃O₃Si
CAS No.:1431322-88-1
Molecular Formula:C₂₃H₃₃N₃O₃Si
Molecular Weight:427.619
Hs Code.:

C<sub>23</sub>H<sub>33</sub>N<sub>3</sub>O<sub>3</sub>Si

Synonyms:C₂₃H₃₃N₃O₃Si

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Chemical Property of C₂₃H₃₃N₃O₃Si

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Technology Process of C₂₃H₃₃N₃O₃Si

There total 12 articles about C₂₃H₃₃N₃O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1431322-88-1
C₂₃H₃₃N₃O₃Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: toluene-4-sulfonic acid / toluene / Reflux; Dean-Stark

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -50 - -40 °C

2.2: 0.5 h / -55 - -45 °C

3.1: potassium hydrogencarbonate / methanol; water / 10 - 50 °C

4.1: potassium tert-butylate / tetrahydrofuran / 1 h / 10 - 60 °C

4.2: 10 - 60 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 50 - 60 °C

6.1: palladium 10% on activated carbon; ammonium formate / methanol; water / 10 - 50 °C / Inert atmosphere

7.1: dichloromethane / 20 - 45 °C

7.2: 20 °C

8.1: Jones reagent / acetone / 2 h / 0 - 37 °C

9.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

9.2: 20 °C

With lithium aluminium tetrahydride; Jones reagent; palladium 10% on activated carbon; potassium tert-butylate; ammonium formate; benzotriazol-1-ol; potassium hydrogencarbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene;

Reference yield:

: 1129634-44-1,1454843-77-6,1454843-78-7
(6S)-5-[(tert-butoxy)carbonyl]-5-azaspiro[2.4]heptane-6-carboxylic acid

: 1431322-87-0
4-((trimethylsilyl)ethynyl)benzene-1,2-diamine

: 1431322-88-1
C₂₃H₃₃N₃O₃Si

Guidance literature:: (6S)-5-[(tert-butoxy)carbonyl]-5-azaspiro[2.4]heptane-6-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

4-((trimethylsilyl)ethynyl)benzene-1,2-diamine; In dichloromethane; at 20 ℃;

Reference yield:

: 958275-39-3
(3R,7aS)-6-methylene-3-phenyltetrahydropyrrolo[1,2-c]oxazol-5(1H)-one

: 1431322-88-1
C₂₃H₃₃N₃O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 10 - 60 °C

1.2: 10 - 60 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 50 - 60 °C

3.1: palladium 10% on activated carbon; ammonium formate / methanol; water / 10 - 50 °C / Inert atmosphere

4.1: dichloromethane / 20 - 45 °C

4.2: 20 °C

5.1: Jones reagent / acetone / 2 h / 0 - 37 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

6.2: 20 °C

With lithium aluminium tetrahydride; Jones reagent; palladium 10% on activated carbon; potassium tert-butylate; ammonium formate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water; acetone;