1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Base Information

Chemical Name:1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane
CAS No.:81279-27-8
Molecular Formula:C₁₉H₂₁NO₄
Molecular Weight:327.38
Hs Code.:

1-<N-(benzyloxycarbonyl)amino>-1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Synonyms:1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Chemical Property:

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Technology Process of 1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

There total 5 articles about 1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20850-43-5
5-(chloromethyl)-1,3-benzodioxole

: 81279-27-8
1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) LDA, hexamethylphosphoramide / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, overnight

2: triethylamine / H₂O; acetone / 0 °C

3: NaN₃ / H₂O; acetone / 0.75 h / Ambient temperature

4: toluene / 0.5 h / Heating

5: Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; triethylamine; lithium diisopropyl amide; In water; acetone; toluene;
DOI:10.1021/jm00347a010

Reference yield:

: 54508-53-1
2,2-dimethyl-3-<3,4-(methylenedioxy)phenyl>propionic acid

: 81279-27-8
1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / H₂O; acetone / 0 °C

2: NaN₃ / H₂O; acetone / 0.75 h / Ambient temperature

3: toluene / 0.5 h / Heating

4: Heating

With sodium azide; triethylamine; In water; acetone; toluene;
DOI:10.1021/jm00347a010

Reference yield:

: C₁₅H₁₈O₆

: 81279-27-8
1--1,1-dimethyl-2-<3,4-(methylenedioxy)phenyl>ethane

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / H₂O; acetone / 0.75 h / Ambient temperature

2: toluene / 0.5 h / Heating

3: Heating

With sodium azide; In water; acetone; toluene;
DOI:10.1021/jm00347a010