5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

Base Information

Chemical Name:5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate
CAS No.:1312698-64-8
Molecular Formula:C₆H₃N₃O₇*C₉H₈N₄OS
Molecular Weight:449.36
Hs Code.:

Synonyms:5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

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Chemical Property of 5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

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Technology Process of 5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

There total 2 articles about 5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312698-63-7
3-amino-6-[2-(2-thienyl)vinyl]-1,2,4-triazin-5(4H)-one

: 88-89-1
2,4,6-Trinitrophenol

: 1312698-64-8
5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

Guidance literature:: In methanol; at 40 ℃; for 0.75h;
DOI:10.1016/j.molstruc.2011.04.001

Reference yield:

: 4-(2-thienyl)-2-oxo-3-butenoic acid

: 1312698-64-8
5-oxo-6-[2-(2-thienyl)vinyl]-4,5-dihydro-1,2,4-triazin-3-aminium-2,4,6-trinitrobenzenolate

Guidance literature:: Multi-step reaction with 2 steps

1: silica gel / methanol; dichloromethane / 0.03 h / Microwave irradiation

2: methanol / 0.75 h / 40 °C

With silica gel; In methanol; dichloromethane;
DOI:10.1016/j.molstruc.2011.04.001