α-(3,4-dimethoxyphenyl)furfuryl alcohol

Base Information

• Chemical Name: α-(3,4-dimethoxyphenyl)furfuryl alcohol
• CAS No.: 134733-96-3
• Molecular Formula: C₁₃H₁₄O₄
• Molecular Weight: 234.252
• Mol file: 134733-96-3.mol

Synonyms:α-(3,4-dimethoxyphenyl)furfuryl alcohol

Chemical Property of α-(3,4-dimethoxyphenyl)furfuryl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-(3,4-dimethoxyphenyl)furfuryl alcohol

There total 1 articles about α-(3,4-dimethoxyphenyl)furfuryl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

furan (110-00-9) + 3,4-dimethoxy-benzaldehyde (120-14-9) → α-(3,4-dimethoxyphenyl)furfuryl alcohol (134733-96-3)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; for 3h; Ambient temperature;

DOI:10.1002/jhet.5570280325

Reference yield: 94.0%

α-(3,4-dimethoxyphenyl)furfuryl alcohol (134733-96-3) + 3,5-Bis-(trifluoromethyl)aniline (328-74-5) → (4R,5S)-4-((3,5-bis(trifluoromethyl)phenyl)amino)-5-(3,4-dimethoxyphenyl)cyclopent-2-enone

Guidance literature:

3,5-Bis-(trifluoromethyl)aniline; With C₄₉H₃₁O₄P; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 0.5h;

α-(3,4-dimethoxyphenyl)furfuryl alcohol; In 1,2-dichloro-ethane; at 20 ℃; for 27h; enantioselective reaction;

DOI:10.1002/anie.201607714

Reference yield: 79.0%

C16H14N2 + α-(3,4-dimethoxyphenyl)furfuryl alcohol (134733-96-3) → 10-(3,4-dimethoxyphenyl)-9a,10,12,12a-tetrahydrobenzo[b]-cyclopenta[f]pyrrolo[1,2-d][1,4]diazepin-11(9H)-one

Guidance literature:

With indium(III) triflate; In acetonitrile; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c5ob01616a

upstream raw materials:

furan

3,4-dimethoxy-benzaldehyde

Downstream raw materials:

2-(3,4-dimethoxyphenyl)-6-hydroxy-2H-pyran-3(6H)-one

1-(3,4-dimethoxyphenyl)-2-hydroxyimino-1,5-pentanodiol

2-(3,4-dimethoxyphenyl)-6-hydroxy-3-hydroxyiminotetrahydro-2H-pyran-3-one

5-acetylamino-6-(3,4-dimethoxyphenyl)-δ-valerolactone