(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

Base Information

Chemical Name:(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate
CAS No.:1354724-81-4
Molecular Formula:C₂₂H₃₂N₂O₄SSe
Molecular Weight:499.533
Hs Code.:

Synonyms:(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

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Chemical Property of (R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

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Technology Process of (R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

There total 4 articles about (R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₄N₂O₅SSe

: 1354724-81-4
(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

Guidance literature:: With silica gel; In toluene; at 20 ℃; for 0.166667h;
DOI:10.1021/ol203237r

Reference yield:

: 104504-02-1
4-methyl-N-(tosyloxy)benzenesulfonamide

: 1354724-81-4
(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate / toluene / 20 h / 20 °C

2: caesium carbonate / toluene / 2 h / 20 °C

3: silica gel / toluene / 0.17 h / 20 °C

With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate; silica gel; caesium carbonate; In toluene;
DOI:10.1021/ol203237r

Reference yield:

: 2463-53-8,18829-56-6,60784-31-8
non-2-enal

: 1354724-81-4
(R)-methyl 2-(dimethylamino)-5-(1-(4-methylphenylsulfonamido)heptyl)selenophene-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate / toluene / 20 h / 20 °C

2: caesium carbonate / toluene / 2 h / 20 °C

3: silica gel / toluene / 0.17 h / 20 °C

With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate; silica gel; caesium carbonate; In toluene;
DOI:10.1021/ol203237r