1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide

Base Information

• Chemical Name: 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide
• CAS No.: 874212-65-4
• Molecular Formula: C₁₆H₂₁N₃O₃
• Molecular Weight: 303.361

Synonyms:1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide

Chemical Property of 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide

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Technology Process of 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide

There total 1 articles about 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1-((3S,4S)-2-Oxo-4-phenoxy-azetidin-3-ylcarbamoyl)-cyclohexyl]-carbamic acid benzyl ester → 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide (874212-65-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 8h; under 2585.74 Torr;

DOI:10.1016/j.bmcl.2004.12.088

Reference yield:

4-(2-(dimethylamino)thiazol-4-yl)benzoic acid (849682-29-7) + 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide (874212-65-4) → 4-(2-Dimethylamino-thiazol-4-yl)-N-[1-((3S,4S)-2-oxo-4-phenoxy-azetidin-3-ylcarbamoyl)-cyclohexyl]-benzamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1016/j.bmcl.2004.12.088

Reference yield:

4-[2-(4-methyl-piperazin-1-yl)-thiazol-4-yl]-benzoic acid (294622-47-2) + 1-Amino-cyclohexanecarboxylic acid ((3S,4S)-2-oxo-4-phenoxy-azetidin-3-yl)-amide (874212-65-4) → 4-[2-(4-Methyl-piperazin-1-yl)-thiazol-4-yl]-N-[1-((3S,4S)-2-oxo-4-phenoxy-azetidin-3-ylcarbamoyl)-cyclohexyl]-benzamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1016/j.bmcl.2004.12.088

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