p-bromophenacyl chloroacetate

Base Information

• Chemical Name: p-bromophenacyl chloroacetate
• CAS No.: 90766-28-2
• Molecular Formula: C₁₀H₈BrClO₃
• Molecular Weight: 291.529
• Mol file: 90766-28-2.mol

Synonyms:p-bromophenacyl chloroacetate

Chemical Property of p-bromophenacyl chloroacetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of p-bromophenacyl chloroacetate

There total 3 articles about p-bromophenacyl chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

chloroacetic acid (79-11-8) + para-bromophenacyl bromide (99-73-0,132309-76-3) → p-bromophenacyl chloroacetate (90766-28-2)

Guidance literature:

With potassium fluoride; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

DOI:10.1021/ac50064a047

Reference yield:

4-bromo-2-hydroxyacetophenone (3343-45-1) + chloroacetic acid (79-11-8) → p-bromophenacyl chloroacetate (90766-28-2)

Guidance literature:

DOI:10.1039/jr9620003204

Reference yield:

→ p-bromophenacyl chloroacetate (90766-28-2)

Guidance literature:

/BRN= 3298640/;

DOI:10.1021/ja01349a501

upstream raw materials:

4-bromo-2-hydroxyacetophenone

chloroacetic acid

para-bromophenacyl bromide

Refernces