(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

Base Information

Chemical Name:(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene
CAS No.:213315-12-9
Molecular Formula:C₁₆H₂₇BrO₂
Molecular Weight:331.293
Hs Code.:

Synonyms:(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

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Chemical Property of (3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

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Technology Process of (3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

There total 1 articles about (3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 109-92-2,25104-37-4
ethyl vinyl ether

: 211503-61-6
(1S,4S,5R,)-(-)-5-Isopropenyl-2,3,4-trimethylcyclohex-2-enol

: 213315-12-9
(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

Guidance literature:: With N-Bromosuccinimide; In dichloromethane; at -50 ℃; for 2h;
DOI:10.1016/S0040-4039(98)01148-4

Reference yield:

: 213315-12-9
(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

: (1S,2R,3R,4R,5R)-2-(2-Hydroxy-ethyl)-5-isopropenyl-2,3,4-trimethyl-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₃SnCl, NaCNBH₃, AIBN; 2.) Jones reagent / 1.) t-BuOH, reflux, 3 h; 2.) Me₂CO, sonication, 4 min

2: LAH / diethyl ether / 2 h / -78 °C

With lithium aluminium tetrahydride; jones reagent; 2,2'-azobis(isobutyronitrile); tributyltin chloride; sodium cyanoborohydride; In diethyl ether;
DOI:10.1016/S0040-4039(98)01148-4

Reference yield:

: 213315-12-9
(3S,4R,6S)-6-(2-Bromo-1-ethoxy-ethoxy)-4-isopropenyl-1,2,3-trimethyl-cyclohexene

: (1S,2R,3S,4R,5R)-2-(2-Hydroxy-ethyl)-5-isopropenyl-2,3,4-trimethyl-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₃SnCl, NaCNBH₃, AIBN; 2.) Jones reagent / 1.) t-BuOH, reflux, 3 h; 2.) Me₂CO, sonication, 4 min

2: LAH / diethyl ether / 2 h / -78 °C

With lithium aluminium tetrahydride; jones reagent; 2,2'-azobis(isobutyronitrile); tributyltin chloride; sodium cyanoborohydride; In diethyl ether;
DOI:10.1016/S0040-4039(98)01148-4