Technology Process of (S)-(-)-p-(2-acetoxy-1-methylethyl)benzyl alcohol
There total 5 articles about (S)-(-)-p-(2-acetoxy-1-methylethyl)benzyl alcohol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver nitrate;
In
water; acetone;
for 3h;
Ambient temperature;
DOI:10.1248/cpb.40.1721
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 490 mg / diethyl ether / 0.5 h / Ambient temperature
2: 94.2 percent / lithium aluminum hydride / diethyl ether / 2 h / Ambient temperature
3: 88.4 percent / pyridine / 1.5 h / 70 - 80 °C
4: 66.4 percent / aluminum chloride / CCl4 / 0.5 h / 0 - 5 °C
5: 53.3 percent / silver nitrate / acetone; H2O / 3 h / Ambient temperature
With
lithium aluminium tetrahydride; aluminium trichloride; silver nitrate;
In
pyridine; tetrachloromethane; diethyl ether; water; acetone;
DOI:10.1248/cpb.40.1721
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94.2 percent / lithium aluminum hydride / diethyl ether / 2 h / Ambient temperature
2: 88.4 percent / pyridine / 1.5 h / 70 - 80 °C
3: 66.4 percent / aluminum chloride / CCl4 / 0.5 h / 0 - 5 °C
4: 53.3 percent / silver nitrate / acetone; H2O / 3 h / Ambient temperature
With
lithium aluminium tetrahydride; aluminium trichloride; silver nitrate;
In
pyridine; tetrachloromethane; diethyl ether; water; acetone;
DOI:10.1248/cpb.40.1721
