(1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

Base Information

Chemical Name:(1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline
CAS No.:114907-43-6
Molecular Formula:C₂₁H₂₀N₂O₃
Molecular Weight:348.401
Hs Code.:

Synonyms:(1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

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Technology Process of (1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

There total 2 articles about (1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 160847-19-8
(1RS)-2-benzyloxycarbonyl-1-(2-hydroxyethyl)-1,2,3,4-tetrahydro-β-carboline

: 114907-43-6
(1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; Ambient temperature;
DOI:10.1055/s-1994-25669

Reference yield:

: 142656-10-8
(1RS)-2-(benzyloxycarbonyl)-1,2,3,4-tetrahydro-1-<(methoxycarbonyl)methyl>-β-carboline

: 114907-43-6
(1RS)-2-benzyloxycarbonyl-1-(2-oxoethyl)-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / LiBH₄ / 1,2-dimethoxy-ethane / 24 h / Ambient temperature

2: 63 percent / molecular sieves 4A, 4-methylmorpholine N-oxide, tetrapropylammonium perruthenate / CH₂Cl₂ / Ambient temperature

With lithium borohydride; tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1055/s-1994-25669