2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

Base Information

Chemical Name:2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride
CAS No.:176895-70-8
Molecular Formula:C₂₉H₃₁ClO₆
Molecular Weight:511.015
Hs Code.:

Synonyms:2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

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Chemical Property of 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

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Technology Process of 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

There total 4 articles about 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 176895-69-5
1,2-di-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranose

: 176895-70-8
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(95)00391-6

Reference yield:

: 2-O-allyl-3,4,6-tri-O-benzyl-D-altropyranose

: 176895-70-8
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 92.1 percent / PdCl₂ / methanol / 4 h / Ambient temperature

2: 100 percent / pyridine / 5 h / Ambient temperature

3: 90 percent / HCl(gas) / diethyl ether / 2 h / Ambient temperature

With pyridine; hydrogenchloride; palladium dichloride; In methanol; diethyl ether;
DOI:10.1016/0008-6215(95)00391-6

Reference yield:

: 176757-50-9
methyl 2-O-allyl-3,4,6-tri-O-benzyl-α-D-altropyranoside

: 176895-70-8
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-altropyranosyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 75.4 percent / aq. AcOH, HCl / 8 h / 95 °C

2: 92.1 percent / PdCl₂ / methanol / 4 h / Ambient temperature

3: 100 percent / pyridine / 5 h / Ambient temperature

4: 90 percent / HCl(gas) / diethyl ether / 2 h / Ambient temperature

With pyridine; hydrogenchloride; acetic acid; palladium dichloride; In methanol; diethyl ether;
DOI:10.1016/0008-6215(95)00391-6