1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin

Base Information

• Chemical Name: 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin
• CAS No.: 1365691-89-9
• Molecular Formula: C₄₇H₅₅N₅O₁₉
• Molecular Weight: 993.976

Synonyms:1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin

Chemical Property of 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin

Chemical Property:

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Technology Process of 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin

There total 1 articles about 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,3,2',7',4-pentakis-N-(benzyloxycarbonyl)apramycin (82002-36-6) → 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin (1365691-89-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 26 ℃; for 4h;

Reference yield: 95.0%

1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin (1365691-89-9) → 7'-N,6'-O-carbonyl-4-N,6-O-carbonyl-apramycin triacetate

Guidance literature:

With 20% palladium hydroxide-activated charcoal; hydrogen; acetic acid; In 1,4-dioxane; water; for 15h; under 760.051 Torr;

Reference yield: 70.0%

1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-4-N-6-O-carbonyl-apramycin (1365691-89-9) → 1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-apramycin (1365691-91-3)

Guidance literature:

With barium hydroxide monohydrate; water; In 1,4-dioxane; at 70 ℃; for 3h;

upstream raw materials:

1,3,2',7',4-pentakis-N-(benzyloxycarbonyl)apramycin

Downstream raw materials:

1,3,2'-tris-N-(benzyloxycarbonyl)-7'-N,6'-O-carbonyl-apramycin

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