2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

Base Information

Chemical Name:2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde
CAS No.:783332-47-8
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

Synonyms:2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

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Chemical Property of 2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

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Technology Process of 2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

There total 3 articles about 2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 311313-44-7
2-(3-methoxy-5-methylphenoxy)tetrahydropyran

: 783332-47-8
2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

Guidance literature:: 2-(3-methoxy-5-methylphenoxy)tetrahydropyran; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at 20 ℃; for 5h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; for 12h;
DOI:10.1021/ja048078t

Reference yield:

: 3209-13-0
O-methylorcinol

: 783332-47-8
2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 97 percent / p-TsOH / tetrahydrofuran / 0 - 20 °C

2.1: tetramethylene diamine; n-butyllithium / tetrahydrofuran; hexane / 5 h / 20 °C

2.2: 100 percent / tetrahydrofuran; hexane / 12 h

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid; In tetrahydrofuran; hexane;
DOI:10.1021/ja048078t

Reference yield:

: 504-15-4
orcinol

: 783332-47-8
2-methoxy-4-methyl-6-tetrahydropyran-2-yloxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / acetone

1.2: NaSC₂H₅ / dimethylformamide

2.1: 97 percent / p-TsOH / tetrahydrofuran / 0 - 20 °C

3.1: tetramethylene diamine; n-butyllithium / tetrahydrofuran; hexane / 5 h / 20 °C

3.2: 100 percent / tetrahydrofuran; hexane / 12 h

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/ja048078t