(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

Base Information

Chemical Name:(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide
CAS No.:1127304-41-9
Molecular Formula:C₄₄H₅₂F₁₇N₃O₉S₂Si
Molecular Weight:1182.1
Hs Code.:

(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

Synonyms:(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

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Chemical Property of (Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

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Technology Process of (Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

There total 1 articles about (Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1127305-25-2
(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-acetoxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

: 1127304-41-9
(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

Guidance literature:: With methanol; ammonia; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200804486

Reference yield:

: 1120367-86-3
diisopropyl((R)-pent-4-en-2-yloxy)silane

: 1127304-41-9
(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

: 1127305-72-9
(Z)-(1'S,4'S,6'S,2''R)-N-{4'-[diisopropyl(pent-4''-en-2''-yloxy)silyloxy]-6'-[tert-butyldimethylsilyloxy]-cyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylbenzenesulfonamido)methylallyloxy]but-2-enyl}-2-nitrobenzenesulfonamide

Guidance literature:: diisopropyl((R)-pent-4-en-2-yloxy)silane; With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

(Z)-(1'S,4'S,6'S)-N-{6'-(tert-butyldimethylsilyloxy)-4'-hydroxycyclohept-2'-en-1'-yl}-N-{4-[2-((N'-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl-4-methylbenzenesulfonamido)methyl)allyloxy]but-2-enyl}-2-nitrobenzenesulfonamide; With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200804486