[(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4]

Base Information

• Chemical Name: [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4]
• CAS No.: 765928-04-9
• Molecular Formula: C₂₈H₅₃NiP₂*C₃₂H₁₂BF₂₄
• Molecular Weight: 1373.59

Synonyms:[(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4]

Chemical Property of [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4]

There total 2 articles about [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMe₂Ph)][B(C₆H₃-3,5-(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro(1,2-bis(di-tert-butylphosphino)ethane)nickel(I) dimer (345893-98-3) → [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH2CMe2Ph)][B(C6H3-3,5-(CF3)2)4] (765928-04-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: tetrahydrofuran

In tetrahydrofuran; diethyl ether;

DOI:10.1021/ja047052z

Reference yield:

neophyl lithium (29904-33-4) → [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH2CMe2Ph)][B(C6H3-3,5-(CF3)2)4] (765928-04-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: tetrahydrofuran

In tetrahydrofuran; diethyl ether;

DOI:10.1021/ja047052z

Reference yield:

[(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH2CMe2Ph)][B(C6H3-3,5-(CF3)2)4] (765928-04-9) → [(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH2CMePhCH2)] (765927-96-6)

Guidance literature:

With NaN(TMS)2; In not given;

DOI:10.1021/ja047052z

upstream raw materials:

chloro(1,2-bis(di-tert-butylphosphino)ethane)nickel(I) dimer

neophyl lithium

Downstream raw materials:

[(1,2-bis(di-tert-butylphosphino)ethane)Ni(CH₂CMePhCH₂)]

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