4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

Base Information

Chemical Name:4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol
CAS No.:941601-16-7
Molecular Formula:C₃₂H₄₃IN₂O₈
Molecular Weight:710.607
Hs Code.:

Synonyms:4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

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Chemical Property of 4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

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Technology Process of 4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

There total 2 articles about 4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 941601-15-6
4β-(2-amino-5-iodobenzoyloxy)-20-ethyl-1α,14α,16β-trimethoxyaconitane-8,9-diol

: 108-24-7
acetic anhydride

: 941601-16-7
4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

Guidance literature:: at 20 - 100 ℃;
DOI:10.1007/s11172-006-0380-2

Reference yield:

: 11033-64-0
N-deacetyllappaconitine

: 941601-16-7
4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / iodine monochloride; acetic acid / 20 - 65 °C

2: 96 percent / 20 - 100 °C

With Iodine monochloride; acetic acid;
DOI:10.1007/s11172-006-0380-2

Reference yield: 86.0%

: 140-76-1,25038-86-2
2-methyl-5-vinylpyridine

: 941601-16-7
4β-[2-(N-acetylamino)-5-iodobenzoyloxy]-1α,14α,16β-trimethoxy-20-ethylaconitane-8,9-diol

: (E)-4β-{2-acetylamino-5-[2-(6-methylpyridin-3-yl)ethenyl]}benzoyloxy-20-ethyl-1α,14α,16β-trimethoxyaconitane-8,9-diol

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1007/s11172-006-0380-2